ASA II Struktur at Universität Greifswald

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Quantitative Messung 2Stk Beispiele

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Probenvorbereitung

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Brom Nachweis

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Carr Price

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Kalibrationsverfahren

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Iod Nachweis

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Qualitative Messung Beispiele 2stk

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Chlor Nachweis

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Analyseverfahren

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Meisenheimer 

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Vitali Morin

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Analysemethode

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Exemplary flashcards for ASA II Struktur at the Universität Greifswald on StudySmarter:

ASA II Struktur

Quantitative Messung 2Stk Beispiele

UV-Vis 

Fluoreszens


=> Lambert Beersches Gesetz => Emissions oder Absorptionsmethoden


ACHTUNG: Quantitative Messung bedeutet immer das Intensität Messsignal proportional zur Kalibrierfunktion 

ASA II Struktur

Probenvorbereitung

  • Lösen der Probe
  • Derivtatisierung (sofern unzugänglich für Messprinzip)
  • Trennung => Erhöhung Sensitivität und Selektivität 
  • Verdünnung oder Anreicherung der Probe 

ASA II Struktur

Brom Nachweis

1. NaCO3

2. HNO3 + AgNO3


=> NS löst sich langsam in Ammoniak

ASA II Struktur

Carr Price

Reagenz:

Antimontrichlorid (SbCl3)


Nachweis: Retinolsäure

ASA II Struktur

Kalibrationsverfahren

Externer Standard

Interner Standard

Standardadditionsverfahren

ASA II Struktur

Iod Nachweis

Erhitzen mit H2SO4 => Violette Dämpfe

ASA II Struktur

Qualitative Messung Beispiele 2stk

NMR

IR

ASA II Struktur

Chlor Nachweis

1. NaCO3

2. HNO3 + AgNO3


NS löst sich schnell in Ammoniak

ASA II Struktur

Analyseverfahren

1. Probenahme


2. Repräsentative Probe (Trennung, Probenvorbereitung) -> Messprobe


3. Messprobe - Messung - Messwerte (Analyseprinzip)


4. Auswertung - Analysenergebnis 


5. Dokumentation

ASA II Struktur

Meisenheimer 

KOH  EthOH

Nitriebarer Aromat oder Aceton

ASA II Struktur

Vitali Morin

HNO3/Hitze

Aceton/KOH

ASA II Struktur

Analysemethode

1. Repräsentative Probe - (Probevorbereitung, Trennung) --> Messprobe 


2. Messprobe - Messung - Messwerte (Analyseprinzip)


3. Auswertung - Analysenergebnis 



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Frabreaktionen ASA

Systematik

04.Pers_Struktur at

Freie Universität Berlin

Infrastruktur at

Technische Hochschule Mittelhessen

Infrastruktur at

Technische Universität Wien

Struktur der at

Szent István University

Struktur & Funktion at

Universität zu Köln

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